Novel X-ray lens facilitates glimpse into the nanoworld

Date:
March 14, 2022
Source:
Paul Scherrer Institute
Summary:
Scientists have developed a ground-breaking achromatic lens
for X-rays.

This allows the X-ray beams to be accurately focused on a single
point even if they have different wavelengths. The new lens will
make it much easier to study nanostructures using X-rays, according
to a new article.



FULL STORY ==========================================================================
PSI scientists have developed a ground-breaking achromatic lens for
X-rays.

This allows the X-ray beams to be accurately focused on a single point
even if they have different wavelengths. The new lens will make it
much easier to study nanostructures using X-rays, according to a paper
just published by the researchers in the scientific journal Nature Communications.


========================================================================== Achromatic lenses are essential for producing sharp images in
photography and optical microscopes. They ensure that different colours
-- i.e. light of different wavelengths -- have a common focal point. To
date, however, achromatic lenses have not been available for X-rays,
so that high-resolution X-ray microscopy has only been possible with monochromatic X-rays. In practice, this means that all other wavelengths
have to be filtered out of the X-ray beam spectrum and hence only a small portion of the light can effectively be used, resulting in a relatively inefficient image capturing process.

A team of PSI scientists have now solved this problem by successfully developing an achromatic X-ray lens for X-rays. Since X-rays can reveal
much smaller structures than visible light, the innovative lens will particularly benefit R&D work in sectors such as microchips, batteries
and materials science, among others.

More complex than in the visible range The fact that it took until now
to develop an achromatic lens for X-rays may at first seem surprising:
for visible light, achromatic lenses have been around for over 200
years. These are usually composed of two different materials. The light penetrates the first material and splits into its spectral colours -
- much like when passing through a conventional glass prism. It then
passes through a second material to reverse this effect. In physics,
the process of separating different wavelengths is called "dispersion."
"This basic principle applied in the visible range does not work in the
X-ray range, however," explains the physicist Christian David, Head of
the X-Ray Optics and Applications research group at PSI's Laboratory for
X-ray Nanoscience and Technologies. "For X-rays, no pair of materials
exists for which the optical properties differ sufficiently over a broad
range of wavelengths for one material to counterbalance the effect of
the other. In other words: the dispersion of materials in the X-ray
range is too similar." Two principles rather than two materials


==========================================================================
So instead of looking for the answer in the combination of two materials,
the scientists linked together two different optical principles. "The
trick was to realise that we could position a second refractive lens in
front of our diffractive lens," says Adam Kubec, lead author of the new
study. Until recently, Kubec was a researcher in Christian David's group,
and now works for XRnanotech, a spin-off that emerged from PSI's research
in X-ray optics.

"For many years now, PSI has been a world leader in the production
of X-ray lenses," says David. "We supply specialised lenses, known as
Fresnel zone plates, for X-ray microscopy at synchrotron light sources worldwide." David's research group uses established nanolithography
methods to produce diffractive lenses. However, for the second element
in the achromatic lens -- the refractive structure -, a new method was
needed which has only recently become available: 3D printing on the
micrometre scale. This ultimately enabled Kubec to produce a shape that
vaguely resembles a miniature rocket.

Potential commercial applications The newly developed lens enables
the leap from research application to X-ray microscopy in commercial
use, for example in industry. "Synchrotron sources generate X-rays of
such high intensity that it is possible to filter out all but a single wavelength while still preserving enough light to produce an image," Kubec explains. However, synchrotrons are large-scale research facilities. To
date, R&D staff working in industry are allocated a set beam time to
conduct experiments at synchrotrons at research institutes, including
the Swiss Light Source SLS at PSI. This beam time is extremely limited, expensive and requires long-term planning. "Industry would like to have
much faster response loops in their R&D processes," Kubec says. "Our
achromatic X- ray lens will help enormously with this: It will enable
compact X-ray microscopes that industrial companies can operate on their
own premises." Together with XRnanotech, PSI plans to market the new
lens. Kubec says they already have suitable contacts with companies specialising in building X-ray microscopy facilities on the lab scale.



==========================================================================
SLS X-ray beam used for testing To characterise their achromatic X-ray
lens, scientists used an X-ray beamline at SLS. One of the methods
employed there is a highly developed X-ray microscopy technique called ptychography. "This technique is normally used to examine an unknown
sample," says the study's second author, Marie-Christine Zdora, a
physicist working in Christian David's research group and an expert in
X-ray imaging. "We on the other hand used ptychography to characterise the
X- ray beam and thus our achromatic lens." This enabled the scientists
to precisely detect the location of the X-ray focal point at different wavelengths.

They additionally tested the new lens using a method where the sample is
moved through the focus of the X-ray beam in small raster steps. When
the wavelength of the X-ray beam is changed, the images produced with
a conventional X-ray lens become very blurred. This, however, does not
happen when using the new achromatic lens. "When we eventually got a
sharp image of the test sample over a broad range of wavelengths, we
knew our lens was working," says a delighted Zdora.

David adds: "The fact that we were able to develop this achromatic X-ray
lens at PSI and will soon be bringing it to market with XRnanotech shows
that the type of research we do here can lead to practical applications
in a very short period of time."

========================================================================== Story Source: Materials provided by Paul_Scherrer_Institute. Original
written by Laura Hennemann. Note: Content may be edited for style
and length.


========================================================================== Journal Reference:
1. Adam Kubec, Marie-Christine Zdora, Umut T. Sanli, Ana Diaz,
Joan Vila-
Comamala, Christian David. An achromatic X-ray lens. Nature
Communications, 2022; 13 (1) DOI: 10.1038/s41467-022-28902-8 ==========================================================================

Link to news story: https://www.sciencedaily.com/releases/2022/03/220314095706.htm

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